Simultaneous Spectrophotometric Determination of Nitrite and Nitrate by Flow Injection Analysis
نویسندگان
چکیده
منابع مشابه
Simultaneous spectrophotometric determination of nitrite and nitrate by flow-injection analysis.
An automatic direct spectrophotometric method for the simultaneous determination of nitrite and nitrate by flow-injection analysis has been developed. Nitrite reacts with 3-nitroaniline in the presence of hydrochloric acid (0.96-1.8 M HCl or pH 0.5-0.7) to form a diazonium cation, which is subsequently coupled with N-(1-naphthyl)-ethylenediamine dihydrochloride to form a stable purple azo dye, ...
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A new rapid flow injection procedure for the simultaneous determination of nitrate, nitrite and ammonium in single flow injection analysis system is proposed. The procedure combines on-line reduction of nitrate to nitrite and oxidation of ammonium to nitrite with spectrophotometric detection of nitrite by using the Griess-Ilosvay reaction. The formed azo dye was measured at 543 nm. The influenc...
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A simple and sensitive flow injection spectrophotometric method is reported for the room temperature determination of nitrite and nitrate based on the Griess reaction and a copperised cadmium column for reduction of nitrate. Calibration graphs were linear over the range 2 – 1000 μg N L (R = 0.9997 and 0.9999, n = 9) with a limit of detection (3 s.d.) of 1.0 μg N L and relative standard deviatio...
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A direct spectrophotometric method has been developed for the sequential determination of nitrite and nitrate by flow injection analysis (FIA). The method is based on the reaction of nitrite with safranine O to form a diazonium salt which caused the reddish-orange dye colour of the solution to be changed to blue in acidic media, and which absorbs at 520 nm. The injected sample in the flow injec...
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A sequential injection analysis (SIA) system for the simultaneous determination of nitrite, nitrate, sulphate and phenolic compounds, in wastewaters has been developed. The nitrite determination is based on the Griess-Llosvay reaction. Nitrate is previously reduced to nitrite in a copperized cadmium column and analyzed as nitrite. The sulphate determination is based on the turbidimetric determi...
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ژورنال
عنوان ژورنال: Analytical Sciences
سال: 2004
ISSN: 0910-6340,1348-2246
DOI: 10.2116/analsci.20.1749